An Aqueous-Based Synthesis of Flower-Like Hydroxy Sodalite Particles in the Presence of Cetyltrimethylammonium bromide
IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata
View Archive InfoField | Value | |
Title |
An Aqueous-Based Synthesis of Flower-Like Hydroxy Sodalite Particles in the Presence of Cetyltrimethylammonium bromide
|
|
Creator |
Naskar, Milan Kanti
Kundu, Debtosh Chatterjee, Minati |
|
Subject |
Processing Science
|
|
Description |
Hydroxy sodalite (HS) particles were synthesized hydrothermally at 90 degrees C for 10 h in the presence of cetyltrimethylammonium bromide (CTAB) and other aqua-based precursor materials like sodium aluminate, sodium metasilicate, and water. Crystalline phases and microstructures of the synthesized particles were studied by X-ray diffraction and field emission scanning electron microscopy, respectively. The effect of CTAB concentrations on the crystallinity and morphology of the synthesized particles was investigated. Thread-ball like HS particles along with some cube-shaped zeolite A were obtained in the presence of 0-0.5 mM CTAB while flower-like HS particles were observed in the presence of 1-5 mM of CTAB concentrations. With increase in CTAB concentration, HS phase increased significantly, and phase pure HS particles resulted for 3 and 5 mM of CTAB concentrations. A mechanism for the formation of flower-like HS particles was also proposed.
|
|
Publisher |
Wiely / American Ceramic Society
|
|
Date |
2011
|
|
Type |
Article
PeerReviewed |
|
Format |
application/pdf
|
|
Identifier |
http://cgcri.csircentral.net/301/1/J_Am_Ceram_Soc_94_[2011_1643%E2%80%931646.pdf
Naskar, Milan Kanti and Kundu, Debtosh and Chatterjee, Minati (2011) An Aqueous-Based Synthesis of Flower-Like Hydroxy Sodalite Particles in the Presence of Cetyltrimethylammonium bromide. Journal of the American Ceramic Society, 94 (6). pp. 1643-1646. ISSN 0002-7820 |
|
Relation |
http://cgcri.csircentral.net/301/
|
|