Annealing behavior of silver, copper, and silver-copper nanoclusters in a silica matrix synthesized by the sol-gel technique
IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata
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Title |
Annealing behavior of silver, copper, and silver-copper nanoclusters in a silica matrix synthesized by the sol-gel technique
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Creator |
De, Goutam
Gusso, M Tapfer, L Catalano, M Gonella, F Mattei, G Mazzoldi, P Battaglin, G |
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Subject |
Microstructure and Characterization
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Description |
Silver, copper, and mixed silver–copper nanocluster-doped silica thin layers were prepared by the sol-gel process. Samples were heat treated in different annealing atmospheres ~air, argon, or 5%H2–95%N2! in the temperature range 500–1100 °C. Specimens were characterized by optical
absorption spectroscopy, Rutherford backscattering spectrometry, x-ray diffraction, and transmission electron microscopy. Cluster growth and dissolution, as well as migration of metal atoms towards the sample surface, with a subsequent evaporation, were observed to occur at temperatures that depend on the annealing atmosphere. In the mixed silver–copper system, the formation of Ag–Cu phase-separated clusters was observed.
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Publisher |
American Institute of Physics
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Date |
1996-12
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Type |
Article
PeerReviewed |
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Format |
application/pdf
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Identifier |
http://cgcri.csircentral.net/1708/1/goutam2.pdf
De, Goutam and Gusso, M and Tapfer, L and Catalano, M and Gonella, F and Mattei, G and Mazzoldi, P and Battaglin, G (1996) Annealing behavior of silver, copper, and silver-copper nanoclusters in a silica matrix synthesized by the sol-gel technique. Journal of Applied Physics, 80 (12). pp. 6734-6739. ISSN 0021-8979 |
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Relation |
http://cgcri.csircentral.net/1708/
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