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Synthesis, consolidation and dielectric properties of BLT ceramics processed by M-PVA gel ignition technique

IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata

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Title Synthesis, consolidation and dielectric properties of BLT ceramics processed by M-PVA gel ignition technique
 
Creator Roy, S
Singh, S
Kumar, P
Bysakh, Sandip
Prasad, V V Bhanu
 
Subject Engineering Materials
 
Description Polycrystalline samples of lanthanum modified bismuth titanate ceramics with composition Bi3.25La0.75Ti3O12 (BLT) were prepared at three different sintering temperatures (1050, 1100 and 1150 degrees C) using M-PVA gel ignition technique. The samples were characterised for structural and electrical properties. A significant amount of as burnt BLT powder was found to be crystalline in nature having a yellowish colour. Very fine BLT nanoparticles were characterised by TEM analysis. Single phase with orthorhombic crystal structure was observed for all the samples, confirmed by X-ray analysis. Dielectric properties were studied as a function of frequency and temperature. More than 95% relative density was observed for all the three sintered samples. The sample sintered at 1100 degrees C showed highest dielectric constant and relative density and lowest loss.
 
Publisher Maney Publishing
 
Date 2013-07
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://cgcri.csircentral.net/2167/1/roy2013.pdf
Roy, S and Singh, S and Kumar, P and Bysakh, Sandip and Prasad, V V Bhanu (2013) Synthesis, consolidation and dielectric properties of BLT ceramics processed by M-PVA gel ignition technique. Advances in Applied Ceramics, 112 (5). pp. 263-269. ISSN 1743-6753
 
Relation http://cgcri.csircentral.net/2167/