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A facile synthesis of Pt nanoflowers composed of an ordered array of nanoparticles

IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata

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Title A facile synthesis of Pt nanoflowers composed of an ordered array of nanoparticles
 
Creator Dandapat, Anirban
Mitra, Anuradha
Gautam, Prateek K
De, Goutam
 
Subject Engineering Materials
 
Description Platinum nanoflowers (Pt NFs) composed of an ordered assembly of nanoparticles were synthesized by an ethanol reduction of [PtCl6](2-) under a reflux condition (85 degrees C) at pH 2.5 in the presence of PVP (molecular weight 10,000) as a structure-directing agent. Optical and transmission electron microscopic (TEM) studies confirmed the reduction of [PtCl6](2-) into Pt-0 followed by its growth to form Pt NPs of a size of similar to 4 nm, which were then assembled into ordered NFs through epitaxial growth along the (111) plane. The mechanism of the Pt NFs' formation with respect to the use of PVP of different molecular weights and the pH of the reaction is discussed in detail.
 
Publisher INTECH
 
Date 2013-07
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://cgcri.csircentral.net/2512/1/dantapat.pdf
Dandapat, Anirban and Mitra, Anuradha and Gautam, Prateek K and De, Goutam (2013) A facile synthesis of Pt nanoflowers composed of an ordered array of nanoparticles. Nanomaterials and Nanotechnology, 3. Article No.-11. ISSN 1847-9804
 
Relation http://cgcri.csircentral.net/2512/