A facile soft-chemical synthesis of cube-shaped mesoporous CuO with microcarpet-like interior
IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata
View Archive Info| Field | Value | |
| Title |
A facile soft-chemical synthesis of cube-shaped mesoporous CuO with microcarpet-like interior
|
|
| Creator |
Ghosh, Sourav
Roy, Mouni Naskar, Milan Kanti |
|
| Subject |
Engineering Materials
|
|
| Description |
Mesoporous cube-shaped CuO with a multishell microcarpet-like patterned interior was synthesized via a facile aqueous-based process using copper nitrate, oxalic acid, and phosphoric acid in the presence of triblock copolymers (TBCs), L64, P123, and F68 at 80 degrees C/2 h followed by calcination at 300-500 degrees C. The obtained products were characterized by differential thermal analysis, thermogravimetry, Fourier transform infrared spectroscopy, Raman spectroscopy, X-ray diffraction, N-2 adsorption-desorption, field emission scanning electron microscopy, and transmission electron microscopy. A possible mechanism for the formation of microcarpet-like patterned interiors in the presence of TBCs as surfactants was illustrated.
|
|
| Publisher |
American Chemical Society
|
|
| Date |
2014-06
|
|
| Type |
Article
PeerReviewed |
|
| Format |
application/pdf
|
|
| Identifier |
http://cgcri.csircentral.net/2592/1/sourav.pdf
Ghosh, Sourav and Roy, Mouni and Naskar, Milan Kanti (2014) A facile soft-chemical synthesis of cube-shaped mesoporous CuO with microcarpet-like interior. Crystal Growth & Design, 14 (6). pp. 2977-2984. ISSN 1528-7483 |
|
| Relation |
http://cgcri.csircentral.net/2592/
|
|