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Growth, structural and microhardness studies of KSb<sub>2</sub>F<sub>7</sub> and KSb<sub>4</sub>F<sub>13</sub> crystals

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Title Growth, structural and microhardness studies of KSb<sub>2</sub>F<sub>7</sub> and KSb<sub>4</sub>F<sub>13</sub> crystals
 
Creator Job, C Besky
Charles, J Benet
 
Subject Microindentation
Hardness
Stiffness constant
 
Description 820-824
Interest in fluoro antimonate crystals have been increased for the last four decades due its super ionic conduction and its unusual electro-optic properties. Optically clear single crystals of KSb<sub>2</sub>F<sub>7</sub> and KSb<sub>4</sub>F<sub>13</sub> were grown by slow evaporation method. Powder X-ray diffraction method has been used for structural identification. The microhardness study shows that hardness steadily increases, then decreases for higher loads. Work hardening coefficient indicates that the grown crystals are moderately softer. Variation of stiffness constant with load for the given crystals has been studied.
 
Date 2011-11-30T12:03:06Z
2011-11-30T12:03:06Z
2011-12
 
Type Article
 
Identifier 0975-1041 (Online); 0019-5596 (Print)
http://hdl.handle.net/123456789/13124
 
Language en_US
 
Rights <img src='http://nopr.niscair.res.in/image/cc-license-sml.png'> <a href='http://creativecommons.org/licenses/by-nc-nd/2.5/in' target='_blank'>CC Attribution-Noncommercial-No Derivative Works 2.5 India</a>
 
Publisher NISCAIR-CSIR, India
 
Source IJPAP Vol.49(12) [December 2011]