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Facile synthesis of higher manganese silicide employing spark plasma assisted reaction sintering with enhanced thermoelectric performance

IR@NPL: CSIR-National Physical Laboratory, New Delhi

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Title Facile synthesis of higher manganese silicide employing spark plasma assisted reaction sintering with enhanced thermoelectric performance
 
Creator Muthiah, Saravanan
Singh, R. C.
Pathak, B. D.
Dhar, Ajay
 
Subject Materials Science
Metallurgy & Metallurgical Engineering
Nanoscience/ Nanotechnology
 
Description This work reports a facile synthesis of aluminium doped higher manganese silicides using a single-step spark plasma assisted in-situ reaction sintering process, which takes only a few minutes as opposed to few hours employing conventional processing methods. Despite employing this cost-effective material processing technique, a figure of merit similar to 0.65 at 873 K was realized, which is comparable to the best value reported thus far. The phase purity, elemental distribution, morphology and structure was investigated employing X-ray diffraction, scanning, transmission electron microscopy and energy dispersive spectroscopy, based on which the thermoelectric performance has been discussed.
 
Publisher Elsevier
 
Date 2016-07-01
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://npl.csircentral.net/2216/1/Facile%20synthesis.pdf
Muthiah, Saravanan and Singh, R. C. and Pathak, B. D. and Dhar, Ajay (2016) Facile synthesis of higher manganese silicide employing spark plasma assisted reaction sintering with enhanced thermoelectric performance. Scripta Materialia, 119. pp. 60-64. ISSN 1359-6462
 
Relation http://npl.csircentral.net/2216/