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Grazing incidence X-ray diffraction (GIRXD) study of the phase composition of SiC (x) Fe (y) and SiC (x) N (y) Fe (z) thin films

IR@NPL: CSIR-National Physical Laboratory, New Delhi

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Title Grazing incidence X-ray diffraction (GIRXD) study of the phase composition of SiC (x) Fe (y) and SiC (x) N (y) Fe (z) thin films
 
Creator Pushkarev, R. V.
Fainer, N. I.
Maurya, K. K.
 
Subject Inorganic Chemistry
Nuclear Chemistry
Physical Chemistry
 
Description Films of various composition are synthesized by chemical vapor deposition under low pressure using the thermal decomposition of the following initial gas mixtures: ferrocene Fe(C5H5)(2) and helium; ferrocene, tris(diethylamino)silane [(C2H5)(2)N](3)SiH (TDEAS) and helium; ferrocene, 1,1,1,3,3,3-hexamethyldisilazane [(CH3)(3)Si](2)NH (HMDS), and helium. The chemical composition of the films obtained is analyzed by FTIR and Raman spectroscopies. The phase composition of the films is studied by grazing incidence X-ray diffraction (GIXRD). It is determined that the films grown from the gas mixtures of organiosilicon compounds (TDEAS or HMDS), ferrocene, and helium have the same chemical and phase composition (SiC (x) N (y) Fe (z) ), while the films obtained from the mixture of ferrocene and helium have another composition (SiC (x) Fe (y) ).
 
Publisher Springer Verlag
 
Date 2016
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://npl.csircentral.net/2233/1/Grazing%20incidence.pdf
Pushkarev, R. V. and Fainer, N. I. and Maurya, K. K. (2016) Grazing incidence X-ray diffraction (GIRXD) study of the phase composition of SiC (x) Fe (y) and SiC (x) N (y) Fe (z) thin films. Journal of Structural Chemistry, 56 (6). 1176-1178 . ISSN 0022-4766
 
Relation http://npl.csircentral.net/2233/