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Synthesis, growth of organic nonlinear optical crystal: Semicarbazone of 2-amino-5-chloro-benzophenone (S2A5CB) and its characterisation

IR@NPL: CSIR-National Physical Laboratory, New Delhi

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Title Synthesis, growth of organic nonlinear optical crystal: Semicarbazone of 2-amino-5-chloro-benzophenone (S2A5CB) and its characterisation
 
Creator Sethuraman, K.
Babu, R. Ramesh
Vijayan, N.
Gopalakrishnan, R.
Ramasamy, P.
 
Subject Crystallography
Materials Science
Applied Physics/Condensed Matter
 
Description A new organic crystal of semicarbazone of 2-amino-5-chloro-benzophenone has been grown as a single crystal by slow evaporation solution growth technique for the first time in the literature. The grown crystal has been characterised by proton nuclear magnetic resonance spectral analysis and single crystal and powder X-ray diffraction studies. Functional groups of the crystallised molecules were confirmed by FT-IR and FT-Raman analyses. Mechanical strength of the crystals was studied by microhardness test. Optical transparency of the grown crystals has been studied by UV-Visible spectra. The second harmonic generation property of the compound was analysed.
 
Publisher Elsevier
 
Date 2006-05-01
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://npl.csircentral.net/2571/1/162.pdf
Sethuraman, K. and Babu, R. Ramesh and Vijayan, N. and Gopalakrishnan, R. and Ramasamy, P. (2006) Synthesis, growth of organic nonlinear optical crystal: Semicarbazone of 2-amino-5-chloro-benzophenone (S2A5CB) and its characterisation. Journal of Crystal Growth, 290 (2). pp. 539-543. ISSN 0022-0248
 
Relation http://npl.csircentral.net/2571/