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Phase determination of ZrB2-B4C ceramic composite material using XRD and rietveld refinement analysis

IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata

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Title Phase determination of ZrB2-B4C ceramic composite material using XRD and rietveld refinement analysis
 
Creator Mandal, Saikat
Pramanick, Ayan
Chakraborty, Shirshendu
Dey, Partha Pratim
 
Subject Engineering Materials
 
Description In this work, the Spark plasma sintering technique has been used to sinter ZrB2-B4C (20 wt%) composite at 2100 degrees C and 50 MPa uniaxial pressure for 15 min soaking in an argon atmosphere. XRD analysis has been carried out on the sintered sample to analyze the different phases present in the ZrB2-B4C composite. The Rietveld refinement technique has been used to analyze the crystal structure, the unit cell information such as space group, cell position, cell angles and atomic distances of the composite material using FULLPROF software. (C) 2019 Elsevier Ltd. All rights reserved.
 
Publisher Elsevier
 
Date 2020-04
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://cgcri.csircentral.net/4963/1/mandal.pdf
Mandal, Saikat and Pramanick, Ayan and Chakraborty, Shirshendu and Dey, Partha Pratim (2020) Phase determination of ZrB2-B4C ceramic composite material using XRD and rietveld refinement analysis. Materials Today-Proceedings, 33 (8). pp. 5664-5666. ISSN 2214-7853
 
Relation http://cgcri.csircentral.net/4963/