CSIR Central

Transesterification of Jatropha curcas Oil by using K Impregnated CaO Heterogeneous Catalyst

IR@CIMFR: CSIR-Central Institute of Mining and Fuel Research, Dhanbad

View Archive Info
 
 
Field Value
 
Title Transesterification of Jatropha curcas Oil by using K Impregnated CaO Heterogeneous Catalyst
 
Creator Sahu, Gajanan
Saha, Sujan
Datta, Sudipta
Chavan, Prakash D
 
Subject Coal Gesification
 
Description Growing environmental concern and fast depletion of conventional fossil fuel resources have induced an urgent search for alternative energy sources. In this regard, biodiesel obtained from Jatropha oil (a non-food oil), seems to be a very promising alternative. Though a lot of research is already done in catalytic transesterification, in the present work, conversion of high FFA (5.5%) bearing Jatropha oil to methyl ester was studied using synthesized KF/CaO solid catalyst. The novelty of this heterogeneous catalyst is the omission of two major steps — neutralization step in which acid is used followed by transesterification using the basic homogeneous catalyst. The catalyst KF/CaO is easily prepared from cheap chemicals and is safe for the environment. The catalyst was characterized by mean of TPD of CO2, X-ray diffraction, BET surface area (SA) analyzer. Catalytic transesterification of this oil was studied with different reaction parameters to achieve a 97% conversion. Optimization of conditions (molar ratio of methanol/oil, time, temperature and catalyst dosage) was also established. The present work makes the process not only safer to the environment but also shows the gateway for greener alternatives to the energy of high FFA oils.
 
Publisher NISCAIR
 
Date 2020-12
 
Type Article
PeerReviewed
 
Identifier Sahu, Gajanan and Saha, Sujan and Datta, Sudipta and Chavan, Prakash D (2020) Transesterification of Jatropha curcas Oil by using K Impregnated CaO Heterogeneous Catalyst. Journal of Scientific & Industrial Research , 79. pp. 1080-1086. ISSN 0022-4456
 
Relation http://cimfr.csircentral.net/2351/