Synthesis and characterization of ferrierite-type zeolite in the presence of nonionic surfactants
Metadata of CSIR Papers
View Archive InfoField | Value | |
Title |
Synthesis and characterization of ferrierite-type zeolite in the presence of nonionic surfactants
|
|
Creator |
Khomane, RB
Kulkarni, BD Ahedi, RK |
|
Subject |
Chemistry, Physical
|
|
Description |
Pure-phase ferrierite (FER) zeolite has been synthesized in the presence of small amounts of nonionic surfactants, Tween 20 and Tween 80. The input SiO2/Al2O3 molar ratio has been varied over a range of 25 to 150. The results confirm that a small amount of pyrrolidine acts as a template and is necessary. The effects of varying concentration of surfactant on ferrierite crystallization and output SiO2/Al2O3 molar ratio are reported. The results also show that in the absence of pyrrolidine, ZSM-5 cocrystallized with FER, whereas in the absence of a nonionic surfactant the yield and crystallization of FER are very poor. The XRF analysis shows the changes in SiO2/Al2O3 output molar ratios as the surfactant concentration changes. The XRD data show that the samples are fully crystalline and pure. The TG/DTA of the sample shows its structural stability. The scanning electron microscopy results show changes in particle size with varying concentration of nonionic surfactant. (C) 2001 Academic Press.
|
|
Publisher |
ACADEMIC PRESS INCSAN DIEGO525 B ST, STE 1900, SAN DIEGO, CA 92101-4495 USA
|
|
Date |
2011-09-24T08:49:39Z
2011-09-24T08:49:39Z 2001 |
|
Type |
Article
|
|
Identifier |
JOURNAL OF COLLOID AND INTERFACE SCIENCE
0021-9797 http://hdl.handle.net/123456789/24083 |
|
Language |
English
|
|