Solid-supported palladium nano and microparticles: an efficient heterogeneous catalyst for ligand-free Suzuki–Miyaura cross coupling reaction
IR@IHBT: CSIR-Institute of Himalayan Bioresource Technology, Palampur
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Title |
Solid-supported palladium nano and microparticles: an efficient heterogeneous
catalyst for ligand-free Suzuki–Miyaura cross coupling reaction
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Creator |
Das, Pralay
Sharma, D Shil, Arun K Kumari, A |
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Subject |
Synthetic Chemistry
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Description |
a b s t r a c t
Solid-supported nano and microparticles of Pd(0) (SS-Pd) were prepared and used as heterogeneous catalysts
for Suzuki–Miyaura cross coupling reactions of aryl halides (chloro, bromo and iodo) and phenyl
boronic acid under mild and ligand-free conditions. Scanning electron microscope (SEM) and UV–vis
based studies were performed to observe the distribution of nano and microparticles of palladium over
solid surface and their oxidation states. In addition, the catalyst could be reused up to seven runs without
significant loss of activity and stable enough under moist conditions.
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Date |
2011
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Type |
Article
PeerReviewed |
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Format |
application/pdf
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Identifier |
http://ihbt.csircentral.net/907/1/TETL38945.pdf
Das, Pralay and Sharma, D and Shil, Arun K and Kumari, A (2011) Solid-supported palladium nano and microparticles: an efficient heterogeneous catalyst for ligand-free Suzuki–Miyaura cross coupling reaction. Tetrahedron Letters, 52. pp. 1176-1178. ISSN |
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Relation |
http://ihbt.csircentral.net/907/
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