Synthesis, characterization and thermal decomposition of M1[M2(C2O4)2].xH2O (x=5 for M1=Co and x=4 for M1=Cd;M2=Ni
IR@NEIST: CSIR-North East Institute of Science and Technology, Jorhat
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Title |
Synthesis, characterization and thermal decomposition of M1[M2(C2O4)2].xH2O (x=5 for M1=Co and x=4 for M1=Cd;M2=Ni
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Creator |
DEB , N
BARUAH , S D DASS , N N |
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Subject |
Chemistry
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Description |
Cobalt bis(oxalato)nickelate pentahydrate, Co[Ni(C2O4)2]×5H2O and cadmium bis(oxalato)nickelate
tetrahydrate, Cd[Ni(C2O4)2]×4H2O have been synthesized and characterized by elemental analysis,
reflectance and IR spectral studies. Thermal decomposition studies (TG, DTG and DTA ) in air
showed that both the compound of cobalt and cadmium produced the oxide, MNiOx (x=3 for M=Co;
x=2 for M=Cd ) at 325 and 360°C respectively. DSC studies in nitrogen attributed only the mixture
of both the metal at the end.
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Date |
2000
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Type |
Article
PeerReviewed |
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Format |
application/pdf
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Identifier |
http://neist.csircentral.net/362/1/918_J_Therm_Anal_Col_2000_59p791%2D97.pdf
DEB , N and BARUAH , S D and DASS , N N (2000) Synthesis, characterization and thermal decomposition of M1[M2(C2O4)2].xH2O (x=5 for M1=Co and x=4 for M1=Cd;M2=Ni. J Thermal Analysis and Calorimetry, 59. pp. 791-797. |
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Relation |
http://neist.csircentral.net/362/
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