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Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications

IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata

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Title Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications
 
Creator Sinha, Mithlesh Kumar
Sen, P S
Basu, Debabrata
 
Subject Ceramic-Metal Systems
 
Description A method is described for preparing dense, polycrystalline beta-tricalcium phosphate. The phase composition of the precipitate made by mixing Ca(OH)(2) and H3PO4 Solutions with subsequent drying and calcining has been studied as a function of initial mixing Ca/P molar ratio. Pure beta-tricalcium phosphate is prepared with initial Ca/P = 1.2 and without any pH control. Effects of milling time of calcined powder on the sintering behavior and microstructural development examined. Grinding for a longer time helps in achieving a relatively high density and fine-grain microstructure at 1200 degrees. The synthesized powder of beta-TCP shows good biocompatibility and no cytotoxicity
 
Publisher Indian Chemical Society
 
Date 2001-08
 
Type Article
PeerReviewed
 
Identifier Sinha, Mithlesh Kumar and Sen, P S and Basu, Debabrata (2001) Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications. Journal of Indian Chemical Society, 78 (8). 386 -388. ISSN 0019-4522
 
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