Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications
IR@CGCRI: CSIR-Central Glass and Ceramic Research Institute, Kolkata
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Title |
Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications
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Creator |
Sinha, Mithlesh Kumar
Sen, P S Basu, Debabrata |
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Subject |
Ceramic-Metal Systems
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Description |
A method is described for preparing dense, polycrystalline beta-tricalcium phosphate. The phase composition of the precipitate made by mixing Ca(OH)(2) and H3PO4 Solutions with subsequent drying and calcining has been studied as a function of initial mixing Ca/P molar ratio. Pure beta-tricalcium phosphate is prepared with initial Ca/P = 1.2 and without any pH control. Effects of milling time of calcined powder on the sintering behavior and microstructural development examined. Grinding for a longer time helps in achieving a relatively high density and fine-grain microstructure at 1200 degrees. The synthesized powder of beta-TCP shows good biocompatibility and no cytotoxicity
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Publisher |
Indian Chemical Society
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Date |
2001-08
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Type |
Article
PeerReviewed |
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Identifier |
Sinha, Mithlesh Kumar and Sen, P S and Basu, Debabrata (2001) Synthesis, sintering and microstructure of beta-tricalcium phosphate for prosthetic applications. Journal of Indian Chemical Society, 78 (8). 386 -388. ISSN 0019-4522
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Relation |
http://cgcri.csircentral.net/790/
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