A Comparative elvaluation of operting conditions for the electrochemical bromination of succinimide
IR@CECRI: CSIR-Central Electrochemical Research Institute, Karaikudi
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| Title |
A Comparative elvaluation of operting conditions for the electrochemical bromination of succinimide
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| Creator |
Krishnamoorthy, S.
Kanakamsrinivasan, R. Noel, M. |
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| Subject |
Electroorganic
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| Description |
Platinum was found to be the electrode of choice for both electrochlorination and bromination of succinimide leading to the formation of N chloro succinimide (NCS) and N bromo succinimide (NBS) respectively. Because of the competitive processes 150% and 285% of theoretical charge has to be passed for bromination and chlorination respectively. 12% (w!v) of succinimide could be used for bromination while only 2% (w!v) of this reactant is optimum for chlorination. Optimum conditions have been evaluated for the process. A maximum yield of 55% and 88% could be achieved for bromination and chlorination of succinimide respectively.
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| Publisher |
Central Electrochemical Research Institute
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| Date |
2000
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| Type |
Article
PeerReviewed |
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| Format |
application/pdf
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| Identifier |
http://cecri.csircentral.net/990/1/34-2000.pdf
Krishnamoorthy, S. and Kanakamsrinivasan, R. and Noel, M. (2000) A Comparative elvaluation of operting conditions for the electrochemical bromination of succinimide. Bulletin of Electrochemistry, 16 (12). pp. 544-550. |
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| Relation |
http://cecri.csircentral.net/990/
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