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Synthesis of fluorine doped tin oxide nanoparticles by sol–gel technique and their characterization

IR@CECRI: CSIR-Central Electrochemical Research Institute, Karaikudi

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Title Synthesis of fluorine doped tin oxide nanoparticles by sol–gel technique and their characterization
 
Creator Senthilkumar, V.
Vickraman, P.
Ravikumar, R.
 
Subject Electrochemical Materials Science
 
Description This article presents novel attempt to synthesis of fluorine doped tin oxide (FTO) nanoparticles by sol–gel technique. The synthesized FTO nanoparticles were obtained after calcination. Temperatures of calcination were 600 and 700 degree C due to identify changes in the particles size growth. A DG/DTA and FTIR study identifies the oxide and formation of the nanopowders. The XRD studies confirm the tetragonal crystallite structure of fluorine doped tin oxide. The TEM image confirms the size of FTO particles in nanoscale. The electrical studies on FTO nanopowders results the decrease in resistivity profile with increasing calcinations. The optical band gap studies for sol–gel synthesis FTO nanoparticles is found to be in the range of 4.11–3.84 eV conforming decreasing optical band gap with increasing calcinating temperatures.
 
Publisher Springer Science+Business Media, LLC
 
Date 2010
 
Type Article
PeerReviewed
 
Format application/pdf
 
Identifier http://cecri.csircentral.net/482/1/2010-100.pdf
Senthilkumar, V. and Vickraman, P. and Ravikumar, R. (2010) Synthesis of fluorine doped tin oxide nanoparticles by sol–gel technique and their characterization. Journal of Sol-Jel Science Technology, 53. pp. 316-321. ISSN 0928-0707
 
Relation http://cecri.csircentral.net/482/